Y. Aoyama, Y. Kuroda, M. Komada, N. Tsuchida, Y. Harada, K. Fukaura
9th International Conference on Technology of Plasticity, ICTP 2008 1467-1470 2008年1月 査読有り
Microstructure and mechanical properties of high nitrogen steels whose chemical composition were Fe-17Cr-12Mn-3Mo-0.2N and that was produced by using metal injection moulding method and nitrogen absorption methods were examined. Especially, we have paid careful attention for nitrogen gas introducing temperature, also we investigated the effect of the grain size on hardness. Sintering was performed at the temperature range of 1050 to 1250 in a vacuum, and then nitrogen gas was introduced. Specimens were held at 1300 for 3hrs under nitrogen atmosphere, and then furnace cooled to 1200. Specimens were held at that temperature for 5hrs to absorb nitrogen and give homogeneous microstructure. After held at 1200, specimens were furnacecooled Finally, they were solution-treated at 1200. To refine grain size, reverse-transformation heat treatment was performed. Porosity of compacts was deeply influenced by gas introducing temperature, and increasing the temperature, porosity decreased and hardness of compacts increased. The strength and elongation of the compact to which nitrogen gas was introduced at 1250was about 1050MPa and 60% , respectively. The SUS316L which has relatively high density similar to the high nitrogen compact and was made by means of MIM showed much lower tensile strength and elongation.